ALBA Synchrotron
The end-station is based on two positioning tables that support the detector and the diffractometer (and the beam-conditioning elements). Both tables have been developed in-house.
Beam conditioning elements
These are the elements immediately in front of the sample, they consist of 12-foil attenuators, x-ray position monitors, slits, slow and fast shutters, and a kapton window.
- Position monitors: both 4-quadrant CVD diamond (DECTRIS)
- 12-foil attenuators (ESRF type)
- Fast shutter (FPS400 CEDRAT)
- Slits (JJ-Xray ESRF type)
Diffractometer (HiDiffX - IRELEC)
Where the sample is to be rotated for data collection. The system includes a high accuracy omega axis (and a mini-kappa) and an on-axis viewing system.
- Vertical rotation axis to reduce gravity effects during sample rotation.
- On-axis viewing system: a digital camera allows instantaneous zooming of the sample.
- <200 nm sphere of confusion
- Mini-kappa goniometer allows reorientation of samples
- Fast exchange between SPINE samples, crystallization plates and serial crystallography sample holders
Automatic Sample Changer (ISARA2 - IRELEC)
The 6-axis robotic arm is used to manipulate both cryosamples and room-temperature crystallization plates.
- The liquid N2 Dewar is able to store up to 464 samples (29 unipucks)
- Room temperature sample capacity is 96 samples (six unipucks)
- Robotic arm to mount/unmount SPINE pins
- Ability to scan low profile Greiner, MRC and Fluidigm crystallization plates
- Barcode reading
- Supports EMBL/ESRF and Unipuck standards
Fluorescence detector
XFlash Detector 410-SA - Bruker to allow anomalous scattering experiments.
PILATUS3 X 6M (100Hz) - Dectris
The main data collection detector is capable of recording up to 100 images per second.
- 425 x 435 mm active area, 6 Mpixels
- 1 Million counts dynamic range (20 bits)
- Delivery May 2023
- Virtually noise free
- Sensor thickness 1000um
- Quantum efficiency at 17.5 KeV 76%
Cryostream: 1000 series - Oxford Cryosystems
- 80K to 400K operation
- <0.1 K stability
Crystal washer
Norhof model 915 LN2 pump allows to clean the ice formed on the crystal surface through a liquid nitrogen stream.
Cryoshutter
Allows remote crystal annealing of the crystal.